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However, there have not yet already been a boronic acid immobilized electrode to selectively detect glucose in a signal-increased method. Thinking about malfunctions of detectors at large sugar amounts, the electrochemical sign must be increased proportionally to the sugar focus. Therefore, we synthesized a brand new diboronic acid by-product and fabricated the derivative-immobilized electrodes for the discerning detection of glucose. We performed cyclic voltammetry and electrochemic