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Outcomes revealed that the agglomeration/aggregation of Au NPs (d = 18 nm) in 0.8 mM HClO4 climbed from 19% to 69per cent over two hours, whereas there clearly was no noticeable granular sediment, and Au NPs tended to agglomerate instead of aggregate irreversibly under typical problems. Hence, the recommended current lifetime-based SNEC could serve as a complementary solution to in situ monitor the agglomeration/aggregation of small-sized NPs in solution during the single-particle a