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dition under the nanocellulose/nanoalumina weight ratio of 10.25 and 0.4 wt% of nanocellulose in aqueous solution. The presence of nanoalumina facilitates the change of microstructure morphologies, the increase of BET specific surface area and the adsorption capacities of NC aerogel. Compared with pure NC aerogel (74.07 ± 1.67, 69.87 ± 1.01, 81.21 ± 3.20, 52.07 ± 1.70, 48.49 ± 1.01, 75.45 ± 3.58 and 87.03 ± 0.46 g g-1 for thiophene, anhydrous ethanol, ethyl acetate, cyclohexane, sesame oil, acetone and dichloromethane, respectively), the NC/Al2O3 ae