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02% for 7 days, excellent repeatability with an RSD of 0.004%, and desired response and recovery time of 95 and 120 s, respectively. The results indicate that the proposed microwave sensor has great potential to achieve high sensitivity and fast response toward methanol gas molecules at room temperature.An efficient synthesis of fused azapolycycles based on (benz)imidazole and pyridine scaffolds has been developed. In all cases, the first nucleophilic addition of (benz)imidazoles to alkynyl bromides in tert-pentyl alcohol can proceed i